Progress in complex combustion field diagnostics based on on-line mass spectrometry technology
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摘要: 燃烧场通常是气−固−液三相耦合的复杂体系，其燃烧诊断结果可支撑提高燃烧效率和降低污染物排放的研究。为了使燃烧诊断结果更加精确，先进的检测方法和检测系统必不可少。在线质谱仪具有灵敏度高、分析速度快、检测范围广等优点，可用于高温、高压等严苛条件下的燃烧场诊断，能够获得更全面的诊断信息。本文对近年来在线质谱仪质量分析器、电离源和取样系统等关键技术的发展概况进行了总结，列举了在线质谱技术在燃烧场火焰产物组分浓度和火焰温度测量中的应用，对在线质谱技术在复杂燃烧场诊断方面面临的挑战和发展前景进行了分析。Abstract: The combustion field is usually a complex system of gas-solid-liquid triphase coupling, and the results obtained from combustion diagnostic can support the researches to improve combustion efficiency and reduce pollutant emissions. In order to make the measurement results more accurate, it is urgent to develop advanced detection methods and detection systems. After several years of development, on-line mass spectrometry has the advantages of high sensitivity, fast analysis speed and wide detection range. It can be used for combustion flow field diagnostics under severe conditions such as high temperature and pressure, and can obtain more comprehensive and sensitive diagnostic information. Firstly, this paper summarized the development of key technologies, e.g., analyzer, ionization source, and sampling systems for on-line mass spectrometry in recent years. Secondly, the applications of on-line mass spectrometry on the measurement of flame component concentration and flame temperature in combustion field were enumerated. On this basis, the challenges and development prospects of the on-line mass spectrometry in complex combustion field diagnostics were summarized, which could provide reference for the relevant researchers.
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图 2 多次反射飞行时间质量分析器的结构示意图
Figure 2. Structure diagrams of multiple reflection time of flight mass analyzers
图 5 基于VUV−Kr灯的高性能电离源技术
Figure 5. High performance ionization source technologies based on VUV-Kr lamp
图 6 石英取样喷嘴的实物图和结构示意图
Figure 6. Photograph and structure diagram of the quartz sampling nozzle
图 7 PVC在共振增强多光子电离源和光电子电离源下的质谱图
Figure 7. Mass spectrum of PVC in a resonance enhanced multiphoton ionization source and photoelectron ionization source
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